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Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
Buchkauf
X-Ray Structure Determination, George H. Stout
- Sprache
- Erscheinungsdatum
- 1989
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- (Hardcover)
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- Titel
- X-Ray Structure Determination
- Untertitel
- A Practical Guide, 2nd Edition
- Sprache
- Englisch
- Autor*innen
- George H. Stout
- Verlag
- Wiley-Interscience
- Erscheinungsdatum
- 1989
- Einband
- Hardcover
- Seitenzahl
- 480
- ISBN10
- 0471607118
- ISBN13
- 9780471607113
- Reihe
- Schlagwörter
- Wissenschaft, Technologie, Physik, Chemie, Wissenschaftliche Theorien, Physikalische Chemie, Kristallographie
- Beschreibung
- Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.